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A concise and efficient concurrent synthesis of 6,11-dihydrodibenzo[b,e]azepines and 5,6,11,12-tetrahydrodibenzo[b,f]azocines and their conversion to 4-oxo-8,13-dihydro-4H-benzo[5,6]azepino[3,2,1-ij]quinoline-5-carboxylates and N-acetyl-5,6,11,12-tetrahydrodibenzo[b,f]azocines: synthetic sequence, spectroscopic characterization and the structures of two products.
Acosta Quintero LM, Palma A, Cobo J, Glidewell C. Acosta Quintero LM, et al. Acta Crystallogr C Struct Chem. 2019 Jun 1;75(Pt 6):650-656. doi: 10.1107/S2053229619005746. Epub 2019 May 15. Acta Crystallogr C Struct Chem. 2019. PMID: 31166916
Monoclinic and orthorhombic forms of (RS)-(E)-4-[2-(4-chlorobenzylidene)hydrazinyl]-6,11-dimethyl-6,11-dihydro-5H-benzo[b]pyrimido[5,4-f]azepine: synthesis, concomitant polymorphism and supramolecular assembly mediated by C-H...N, C-H...π(arene) and C-Cl...π(arene) interactions.
Acosta Quintero LM, Palma A, Choquesillo-Lazarte D, Cobo J, Glidewell C. Acosta Quintero LM, et al. Acta Crystallogr C Struct Chem. 2019 Jun 1;75(Pt 6):686-693. doi: 10.1107/S205322961900617X. Epub 2019 May 17. Acta Crystallogr C Struct Chem. 2019. PMID: 31166920