Rentel C - Search Results

1

Detecting the Major Degradation Products of Phosphorothioate Oligonucleotides by Chemical Derivatization and Weak Anion Exchange Chromatography.

Roussis SG, Gabriel CM, Rodriguez AA, Rentel C. Roussis SG, et al. Among authors: rentel c. ACS Omega. 2024 Nov 19;9(48):47822-47830. doi: 10.1021/acsomega.4c08543. eCollection 2024 Dec 3. ACS Omega. 2024. PMID: 39651088 Free PMC article.

2

Characterizing the Diastereoisomeric Distribution of Phosphorothioate Oligonucleotides by Metal Ion Complexation Chromatography, In-Series Reversed Phase-Strong Anion Exchange Chromatography, and ³¹P NMR.

Roussis SG, Cedillo I, Rentel C. Roussis SG, et al. Among authors: rentel c. Anal Chem. 2021 Dec 7;93(48):16035-16042. doi: 10.1021/acs.analchem.1c03593. Epub 2021 Nov 23. Anal Chem. 2021. PMID: 34813705

3

Rapid Oligonucleotide Drug Impurity Determination by Direct Spectral Comparison of Ion Pair-Reversed Phase HPLC ESI MS Data.

Roussis SG, Koch C, Capaldi D, Rentel C. Roussis SG, et al. Among authors: rentel c. Rapid Commun Mass Spectrom. 2018 Mar 25. doi: 10.1002/rcm.8125. Online ahead of print. Rapid Commun Mass Spectrom. 2018. PMID: 29575209

4

Semi-quantitative determination of co-eluting impurities in oligonucleotide drugs using ion-pair reversed-phase liquid chromatography mass spectrometry.

Roussis SG, Cedillo I, Rentel C. Roussis SG, et al. Among authors: rentel c. J Chromatogr A. 2019 Jan 11;1584:106-114. doi: 10.1016/j.chroma.2018.11.034. Epub 2018 Nov 20. J Chromatogr A. 2019. PMID: 30473112

5

Small alkyl amines as ion-pair reagents for the separation of positional isomers of impurities in phosphate diester oligonucleotides.

Roussis SG, Pearce M, Rentel C. Roussis SG, et al. Among authors: rentel c. J Chromatogr A. 2019 Jun 7;1594:105-111. doi: 10.1016/j.chroma.2019.02.026. Epub 2019 Feb 12. J Chromatogr A. 2019. PMID: 30819437

6

Determination of oligonucleotide deamination by high resolution mass spectrometry.

Rentel C, DaCosta J, Roussis S, Chan J, Capaldi D, Mai B. Rentel C, et al. J Pharm Biomed Anal. 2019 Sep 5;173:56-61. doi: 10.1016/j.jpba.2019.05.012. Epub 2019 May 6. J Pharm Biomed Anal. 2019. PMID: 31121454

7

Assay determination by mass spectrometry for oligonucleotide therapeutics.

Madsen M, Roussis S, Schniepp E, Rentel C, Capaldi D. Madsen M, et al. Among authors: rentel c. Rapid Commun Mass Spectrom. 2019 Nov 30;33(22):1774-1780. doi: 10.1002/rcm.8516. Rapid Commun Mass Spectrom. 2019. PMID: 31278794

8

Automated determination of early eluting oligonucleotide impurities using ion-pair reversed-phase liquid chromatography high resolution-mass spectrometry.

Roussis SG, Cedillo I, Rentel C. Roussis SG, et al. Among authors: rentel c. Anal Biochem. 2020 Apr 15;595:113623. doi: 10.1016/j.ab.2020.113623. Epub 2020 Feb 14. Anal Biochem. 2020. PMID: 32067983

9

Determination of individual oligonucleotide impurities by small amine ion pair-RP HPLC MS and MS/MS: n - 1 impurities.

Roussis SG, Rodriguez AA, Rentel C. Roussis SG, et al. Among authors: rentel c. J Chromatogr B Analyt Technol Biomed Life Sci. 2021 Apr 15;1169:122611. doi: 10.1016/j.jchromb.2021.122611. Epub 2021 Mar 1. J Chromatogr B Analyt Technol Biomed Life Sci. 2021. PMID: 33706187

10

Separation of phosphorothioate oligonucleotide impurities by WAX HPLC under high organic content elution conditions.

Roussis SG, Rentel C. Roussis SG, et al. Among authors: rentel c. Anal Biochem. 2022 Dec 15;659:114956. doi: 10.1016/j.ab.2022.114956. Epub 2022 Oct 18. Anal Biochem. 2022. PMID: 36270331

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