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A novel crystallization-induced diastereomeric transformation based on a reversible carbon-sulfur bond formation. Application to the synthesis of a gamma-secretase inhibitor.
Davies AJ, Scott JP, Bishop BC, Brands KM, Brewer SE, Dasilva JO, Dormer PG, Dolling UH, Gibb AD, Hammond DC, Lieberman DR, Palucki M, Payack JF. Davies AJ, et al. Among authors: bishop bc. J Org Chem. 2007 Jun 22;72(13):4864-71. doi: 10.1021/jo0705925. Epub 2007 May 24. J Org Chem. 2007. PMID: 17521199