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Stereochemical Definition of the Natural Product (6R,10R,13R, 14R,16R,17R,19S,20S,21R,24S,25S,28S,30S,32R,33R,34R,36S,37S,39R)-Azaspiracid-3 by Total Synthesis and Comparative Analyses.
Kenton NT, Adu-Ampratwum D, Okumu AA, McCarron P, Kilcoyne J, Rise F, Wilkins AL, Miles CO, Forsyth CJ. Kenton NT, et al. Among authors: forsyth cj. Angew Chem Int Ed Engl. 2018 Jan 15;57(3):810-813. doi: 10.1002/anie.201711008. Epub 2017 Dec 15. Angew Chem Int Ed Engl. 2018. PMID: 29193497
Total Synthesis of (6R,10R,13R,14R,16R,17R,19S,20R,21R,24S, 25S,28S,30S,32R,33R,34R,36S,37S,39R)-Azaspiracid-3 Reveals Non-Identity with the Natural Product.
Kenton NT, Adu-Ampratwum D, Okumu AA, Zhang Z, Chen Y, Nguyen S, Xu J, Ding Y, McCarron P, Kilcoyne J, Rise F, Wilkins AL, Miles CO, Forsyth CJ. Kenton NT, et al. Among authors: forsyth cj. Angew Chem Int Ed Engl. 2018 Jan 15;57(3):805-809. doi: 10.1002/anie.201711006. Epub 2017 Dec 13. Angew Chem Int Ed Engl. 2018. PMID: 29193614
Synthesis of the C1-C19 Domain of Azaspiracid-34.
Okumu AA, Forsyth CJ. Okumu AA, et al. Among authors: forsyth cj. Org Lett. 2019 Jan 18;21(2):356-359. doi: 10.1021/acs.orglett.8b03451. Epub 2019 Jan 2. Org Lett. 2019. PMID: 30601015
Synthesis of the C22-C40 Domain of the Azaspiracids.
Zhang Z, Chen Y, Adu-Ampratwum D, Okumu AA, Kenton NT, Forsyth CJ. Zhang Z, et al. Among authors: forsyth cj. Org Lett. 2016 Apr 15;18(8):1824-7. doi: 10.1021/acs.orglett.6b00557. Epub 2016 Apr 4. Org Lett. 2016. PMID: 27043010
Development of an ELISA for the Detection of Azaspiracids.
Samdal IA, Løvberg KE, Briggs LR, Kilcoyne J, Xu J, Forsyth CJ, Miles CO. Samdal IA, et al. Among authors: forsyth cj. J Agric Food Chem. 2015 Sep 9;63(35):7855-61. doi: 10.1021/acs.jafc.5b02513. Epub 2015 Aug 26. J Agric Food Chem. 2015. PMID: 26245830
Preparation and characterization of an immunoaffinity column for the selective extraction of azaspiracids.
Samdal IA, Sandvik M, Vu J, Sukenthirarasa MS, Kanesamurthy S, Løvberg KLE, Kilcoyne J, Forsyth CJ, Wright EJ, Miles CO. Samdal IA, et al. Among authors: forsyth cj. J Chromatogr B Analyt Technol Biomed Life Sci. 2022 Sep 1;1207:123360. doi: 10.1016/j.jchromb.2022.123360. Epub 2022 Jul 7. J Chromatogr B Analyt Technol Biomed Life Sci. 2022. PMID: 35839625 Free article.
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