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Development of a large scale asymmetric synthesis of the glucocorticoid agonist BI 653048 BS H3PO4.
Reeves JT, Fandrick DR, Tan Z, Song JJ, Rodriguez S, Qu B, Kim S, Niemeier O, Li Z, Byrne D, Campbell S, Chitroda A, DeCroos P, Fachinger T, Fuchs V, Gonnella NC, Grinberg N, Haddad N, Jäger B, Lee H, Lorenz JC, Ma S, Narayanan BA, Nummy LJ, Premasiri A, Roschangar F, Sarvestani M, Shen S, Spinelli E, Sun X, Varsolona RJ, Yee N, Brenner M, Senanayake CH. Reeves JT, et al. Among authors: shen s. J Org Chem. 2013 Apr 19;78(8):3616-35. doi: 10.1021/jo400079z. Epub 2013 Apr 1. J Org Chem. 2013. PMID: 23544738
Zinc catalyzed and mediated asymmetric propargylation of trifluoromethyl ketones with a propargyl boronate.
Fandrick DR, Reeves JT, Bakonyi JM, Nyalapatla PR, Tan Z, Niemeier O, Akalay D, Fandrick KR, Wohlleben W, Ollenberger S, Song JJ, Sun X, Qu B, Haddad N, Sanyal S, Shen S, Ma S, Byrne D, Chitroda A, Fuchs V, Narayanan BA, Grinberg N, Lee H, Yee N, Brenner M, Senanayake CH. Fandrick DR, et al. Among authors: shen s. J Org Chem. 2013 Apr 19;78(8):3592-615. doi: 10.1021/jo400080y. Epub 2013 Apr 1. J Org Chem. 2013. PMID: 23544787
A superior method for the reduction of secondary phosphine oxides.
Busacca CA, Lorenz JC, Grinberg N, Haddad N, Hrapchak M, Latli B, Lee H, Sabila P, Saha A, Sarvestani M, Shen S, Varsolona R, Wei X, Senanayake CH. Busacca CA, et al. Among authors: shen s. Org Lett. 2005 Sep 15;7(19):4277-80. doi: 10.1021/ol0517832. Org Lett. 2005. PMID: 16146406
On the racemization of chiral imidazolines.
Busacca CA, Bartholomeyzik T, Cheekoori S, Grinberg N, Lee H, Ma S, Saha A, Shen S, Senanayake CH. Busacca CA, et al. Among authors: shen s. J Org Chem. 2008 Dec 19;73(24):9756-61. doi: 10.1021/jo8024384. J Org Chem. 2008. PMID: 19053584
8,690 results