Abstract
New cysteine proteinase inhibitors, TMC-52A, B, C, and D, were isolated from the fungal fermentation broth. On the basis of a taxonomical study, the producing strain, F-2665, was characterized as Gliocladium sp. Spectroscopic analyses and chemical degradation have shown TMC-52A to D to be epoxysuccinyl peptides. TMC-52A to D strongly inhibited cysteine proteinases, in particular, cathepsin L with IC50 values of 13 nM, 10nM, 10nM, and 6nM, respectively.
MeSH terms
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Cathepsin L
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Cathepsins / antagonists & inhibitors*
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Cysteine Endopeptidases
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Cysteine Proteinase Inhibitors* / biosynthesis
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Cysteine Proteinase Inhibitors* / chemistry
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Cysteine Proteinase Inhibitors* / isolation & purification
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Cysteine Proteinase Inhibitors* / pharmacology
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Endopeptidases*
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Magnetic Resonance Spectroscopy
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Mass Spectrometry
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Mitosporic Fungi / chemistry*
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Mitosporic Fungi / classification
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Mitosporic Fungi / metabolism
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Molecular Structure
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Phenylalanine / analogs & derivatives*
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Phenylalanine / chemical synthesis
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Phenylalanine / chemistry
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Phenylalanine / isolation & purification
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Phenylalanine / pharmacology
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Succinates* / chemical synthesis
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Succinates* / chemistry
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Succinates* / isolation & purification*
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Succinates* / pharmacology
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Tyrosine / analogs & derivatives*
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Tyrosine / chemical synthesis
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Tyrosine / chemistry
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Tyrosine / isolation & purification*
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Tyrosine / pharmacology
Substances
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Cysteine Proteinase Inhibitors
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Succinates
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TMC 52A
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TMC 52B
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TMC 52C
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TMC 52D
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Tyrosine
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Phenylalanine
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Cathepsins
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Endopeptidases
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Cysteine Endopeptidases
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Cathepsin L