A method of measuring dipalmitoylphosphatidylcholine (DPPC) by high-performance liquid chromatography (HPLC): effect of dexamethasone on DPPC secretion in fetal rat alveolar type II cell culture

J Obstet Gynaecol Res. 1996 Oct;22(5):481-8. doi: 10.1111/j.1447-0756.1996.tb01061.x.

Abstract

Objective: To establish a method by which to measure dipalmitoylphosphatidylcholine (DPPC), which is the most prevalent phospholipid in lung surfactant, by high-performance liquid chromatography (HPLC), and to measure DPPC secretion in type-II alveolar cell culture to determine whether glucocorticoid has a direct accerelating effect.

Method: Type-II alveolar cell suspensions were made with fetal rat lungs and then cultured. Dexamethasone, (10(-9), 10(-8) M) was added to some of the culture dishes. DPPC was extracted from the culture medium, purified, and measured by high-performance liquid chromatography (HPLC).

Results: In the measurements of DPPC, the specificity of isolation and measurement parity were excellent [coefficient of variation: intraassay; 5.66% (0.005 mg/ml), 25.37% (0.05 mg/ml): interassay; 8.35% (0.005 mg/ml), 0.08% (0.05 mg/ml)]. The DPPC concentration in the culture dishes of the dexamethasone was not significantly different than that of the control dishes (Student's t-test).

Conclusion: The above results prove that dexamethasone does not directly stimulate lung alveolar type-II cells.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • 1,2-Dipalmitoylphosphatidylcholine / analysis
  • 1,2-Dipalmitoylphosphatidylcholine / metabolism*
  • Animals
  • Cells, Cultured
  • Chromatography, High Pressure Liquid*
  • Dexamethasone / pharmacology*
  • Female
  • Pregnancy
  • Pulmonary Alveoli / drug effects
  • Pulmonary Alveoli / embryology*
  • Pulmonary Alveoli / metabolism*
  • Rats
  • Rats, Wistar

Substances

  • 1,2-Dipalmitoylphosphatidylcholine
  • Dexamethasone