Kinetic analysis of synthetic analogues of linear-epitope peptides of glycoprotein D of herpes simplex virus type 1 by surface plasmon resonance

Eur J Biochem. 1996 Aug 15;240(1):209-14. doi: 10.1111/j.1432-1033.1996.0209h.x.

Abstract

The interaction between mAb A16 and glycoprotein D (gD) of herpes simplex virus type 1 was analyzed by studying the kinetics of binding with a surface-plasmon-resonance biosensor. mAb A16 belongs to group VII antibodies, which recognize residues 11-19 of gD. In a previous study, three critical residues, Asp13, Arg16 and Phe17, of this epitope were identified by screening a phage display library that contained a random 15-amino-acid insert with the antibody. The contribution to binding of these residues in the motif DXXRF was further analyzed by an amino-acid-replacement study of the epitope gD-(9-19)-peptide and of a gD-(9-19)-peptide mimotope, previously obtained by screening the phage display library. Amino acid residues of the motif were replaced by a neutral amino acid residue, an amino acid residue with opposite charge and a corresponding D-amino acid residue. Kinetic parameters of peptide analogues were determined with a surface plasmon-resonance biosensor. The kinetic parameters of the peptide analogues were compared with the kinetic parameters of the interaction between mAb A16 and the epitope gD-(9-19)-peptide. The minimal size of the gD epitope for mAb A16 was also determined in this study. The kinetic constants of the resulting gD-(11-17)-peptide were found to be similar to those of entire gD. The kinetic analysis precisely defined the epitope on gD for mAb A16 to residues 11-17, identified Arg16 as an essential residue and suggested that Asp13 and Phe17 are mainly involved in stabilization of the secondary structure of the peptide.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Antibodies, Monoclonal
  • Antigen-Antibody Complex
  • Cell Line
  • Cloning, Molecular
  • Epitopes / chemistry
  • Kinetics
  • Magnetic Resonance Spectroscopy
  • Mutagenesis, Site-Directed
  • Peptide Fragments / chemical synthesis
  • Peptide Fragments / chemistry
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / immunology
  • Simplexvirus
  • Spodoptera
  • Transfection
  • Viral Envelope Proteins / chemistry*
  • Viral Envelope Proteins / immunology

Substances

  • Antibodies, Monoclonal
  • Antigen-Antibody Complex
  • Epitopes
  • Peptide Fragments
  • Recombinant Proteins
  • Viral Envelope Proteins
  • glycoprotein I, herpes simplex virus type 1