Cordil reversibly inhibits the Na,K-ATPase from outside of the cell membrane. Role of K-dependent dephosphorylation

J Recept Res. 1993;13(7):1083-92. doi: 10.3109/10799899309063265.

Abstract

Cordil-LND796 is a new cardiotonic glycoside under development. In rat brain microsomes where three isoforms of the Na,K-ATPase with differential affinities for cardiac glycosides have been identified, Cordil had higher affinity for the alpha 3 (IC50 = 0.02 microM) than for the alpha 2 (IC50 = 0.6 microM) and the alpha 1 (IC50 = 30 microM) isozymes. Cordil is potentially a selective inhibitor for both alpha 2 and alpha 3 Na,K-ATPase isoforms. Using inside out vesicles we have shown that Cordil binds to and inhibits Na,K-ATPase at an extracellular site. The dissociation kinetic rates (k-1) from the ATPase and the phosphatase activity (K-dependent dephosphorylation) of the Na,K-ATPase were similar for Cordil. Despite these similarities to ouabain comparison of the kinetics of the Na,K-ATPase inhibition by ouabain and Cordil revealed marked differences in their association rates (k+1 = 0.7 l mol-1 min-1 and k+1 = 6 x 10(-3) l mol-1 min-1 respectively) and their dissociation rates (k-1 = 1.3 +/- 0.2 x 10(-4) s-1 and k-1 = 69 +/- 7 x 10(-4) s-1 respectively). Both binding association and dissociation rates were enhanced for Cordil. These data are compatible with a stabilizing effect of Cordil on the E2P conformational state of Na,K-ATPase.

MeSH terms

  • Animals
  • Cardiotonic Agents / metabolism
  • Cardiotonic Agents / pharmacology*
  • Dogs
  • Ouabain / metabolism
  • Phosphorylation
  • Potassium / physiology
  • Protein Conformation
  • Rats
  • Sodium-Potassium-Exchanging ATPase / antagonists & inhibitors*
  • Steroids

Substances

  • Cardiotonic Agents
  • Steroids
  • LND 796
  • Ouabain
  • Sodium-Potassium-Exchanging ATPase
  • Potassium