Synthesis of highly diversified carrier ampholytes. Evaluation of the resolving power of isoelectric focusing in the Pi system (alpha-1-antitrypsin genetic polymorphism)

J Chromatogr. 1979 Aug 1;176(1):89-101. doi: 10.1016/s0021-9673(00)92089-2.

Abstract

The use of condensing reagents such as epoxypropanol, diepoxyoctane, acrylamide and N,N'-methylenebisacrylamide in the synthesis of carrier ampholytes increased the diversity of amphoteric components. The quality of these synthetic carrier ampholytes has been tested in the separation of variants of alpha-1-anti-trypsin, a genetic polymorphism called the Pi system. A resolving power of the order of 0.005 pH unit was obtained.

MeSH terms

  • Ampholyte Mixtures / chemical synthesis*
  • Buffers / chemical synthesis*
  • Hydrogen-Ion Concentration
  • Isoelectric Focusing
  • Phenotype
  • Polymorphism, Genetic
  • alpha 1-Antitrypsin / genetics
  • alpha 1-Antitrypsin / isolation & purification*

Substances

  • Ampholyte Mixtures
  • Buffers
  • alpha 1-Antitrypsin