Scutellarein Inhibits Osteosarcoma Growth by Targeting the TLR4/TRAF6/NF-κB Pathway

Drug Des Devel Ther. 2025 Jan 6:19:51-64. doi: 10.2147/DDDT.S489092. eCollection 2025.

Abstract

Purpose: Osteosarcoma (OS) is the most common malignant tumor associated with poor patient outcomes and a limited availability of therapeutic agents. Scutellarein (SCU) is a monomeric flavone bioactive compound with potent anti-cancer activity. However, the effects and mechanisms of SCU on the growth of OS remain unknown.

Methods: The Cell Counting Kit-8, colony formation assay and 5-ethynyl-2'-deoxyuridine (EdU) incorporation assays were used to analyze cell proliferation ability in vitro. TLR4/TRAF6/NF-κB signaling transduction was investigated by RNA sequencing analysis, quantitative real-time polymerase chain reaction, Western blotting, NF-κB luciferase reporter assay, immunofluorescent staining, and immunoprecipitation. Molecular docking and cellular thermal shift assay were employed to confirm the binding interaction between SCU and TLR4. The effects of SCU and TLR4 overexpression on OS growth were analyzed using a xenograft tumor model and immunohistochemical staining.

Results: SCU was found to significantly inhibit OS cell proliferation, and RNA sequencing analysis suggested that the NF-κB pathway is closely associated with this process. Further studies revealed that SCU inhibited the canonical NF-κB pathway through its binding with TLR4, which disrupted the interaction of TLR4 and TRAF6. Moreover, SCU also repressed NF-κB signal transduction by inhibiting TLR4 expression. Furthermore, SCU was revealed to suppress OS cell proliferation by targeting TLR4 in vitro and in vivo.

Conclusion: SCU exhibited a dual impact by inhibiting TLR4 expression and disrupting TLR4-TRAF6 interaction, resulting in NF-κB inactivation, thereby blocking OS growth.

Keywords: NF-κB pathway; TLR4; molecular modeling; osteosarcoma; scutellarein.

MeSH terms

  • Animals
  • Antineoplastic Agents / chemistry
  • Antineoplastic Agents / pharmacology
  • Apigenin* / chemistry
  • Apigenin* / pharmacology
  • Bone Neoplasms / drug therapy
  • Bone Neoplasms / metabolism
  • Bone Neoplasms / pathology
  • Cell Proliferation* / drug effects
  • Dose-Response Relationship, Drug
  • Drug Screening Assays, Antitumor
  • Humans
  • Intracellular Signaling Peptides and Proteins
  • Mice
  • Mice, Inbred BALB C
  • Mice, Nude
  • Molecular Docking Simulation
  • NF-kappa B* / antagonists & inhibitors
  • NF-kappa B* / metabolism
  • Neoplasms, Experimental / drug therapy
  • Neoplasms, Experimental / metabolism
  • Neoplasms, Experimental / pathology
  • Osteosarcoma* / drug therapy
  • Osteosarcoma* / metabolism
  • Osteosarcoma* / pathology
  • Signal Transduction / drug effects
  • Structure-Activity Relationship
  • TNF Receptor-Associated Factor 6 / antagonists & inhibitors
  • TNF Receptor-Associated Factor 6 / metabolism
  • Toll-Like Receptor 4* / antagonists & inhibitors
  • Toll-Like Receptor 4* / metabolism
  • Tumor Cells, Cultured

Substances

  • NF-kappa B
  • Toll-Like Receptor 4
  • TLR4 protein, human
  • Apigenin
  • scutellarein
  • TNF Receptor-Associated Factor 6
  • Antineoplastic Agents
  • Tifab protein, human
  • Intracellular Signaling Peptides and Proteins

Grants and funding

This work was supported by the Traditional Chinese Medicine Science and Technology Project of Shandong Province (2021Q085), the High level scientific research program cultivation project of Jining Medical College (JYGC2021FKJ007) and was a Key R&D project of Jining City (2023YXNS084, 2022YXNS041).