In vivo antitumor activity of PHT-427 inhibitor-loaded polymeric nanoparticles in head and neck squamous cell carcinoma

Drug Deliv. 2025 Dec;32(1):2449376. doi: 10.1080/10717544.2024.2449376. Epub 2025 Jan 9.

Abstract

Recent studies on head and neck squamous cell carcinoma (HNSCC) tumorigenesis have revealed several dysregulated molecular pathways. The phosphatidylinositol-3-kinase (PI3K) signaling pathway is frequently activated in HNSCC, making it an attractive target for therapies. PHT-427 is a dual inhibitor of PI3K and the mammalian target of AKT/PDK1. This study evaluates the anticancer efficacy of the inhibitor PHT-427 loaded into polymeric nanoparticles (NP) based on α-TOS (NP-427) administered by intratumoral injection into a hypopharyngeal squamous cell carcinoma (FaDu cells) heterotopic xenograft mouse model. The nanocarrier system, based on block copolymers of N-vinylpyrrolidone (VP) and a methacrylic derivative of α-TOS (MTOS), was synthesized, and PHT-427 was loaded into the delivery system. First, we evaluated the effect of NP-427 on tumor growth by measuring tumor volume, mouse weight, survival, and the development of tumor ulceration and necrosis. In addition, we measured PI3KCA/AKT/PDK1 gene expression, PI3KCA/AKT/PDK1 protein levels, Epidermal Growth Factor Receptor (EGFR), and angiogenesis in the tumor tissue. PHT-427 encapsulation increased drug efficacy and safety, as demonstrated by decreased tumor volume, reduced PI3K/AKT/PDK1 pathway expression, and improved antitumor activity and necrosis induction in the mouse xenograft model. EGFR and angiogenesis marker (Factor VIII) expression were significantly lower in the NP-427 group compared to other experimental groups. Administration of encapsulated PHT-427 at the tumor sites proves promising for HNSCC therapy.

Keywords: PHT-427 inhibitor; PI3K pathway; hypopharyngeal squamous cell carcinoma; polymeric nanoparticle; tumor xenograft mouse model.

MeSH terms

  • Animals
  • Antineoplastic Agents* / administration & dosage
  • Antineoplastic Agents* / pharmacology
  • Carcinoma, Squamous Cell / drug therapy
  • Cell Line, Tumor
  • Drug Carriers / chemistry
  • ErbB Receptors / antagonists & inhibitors
  • Head and Neck Neoplasms* / drug therapy
  • Humans
  • Mice
  • Mice, Inbred BALB C
  • Mice, Nude
  • Nanoparticles* / chemistry
  • Phosphoinositide-3 Kinase Inhibitors / administration & dosage
  • Phosphoinositide-3 Kinase Inhibitors / pharmacology
  • Polymers* / chemistry
  • Proto-Oncogene Proteins c-akt / metabolism
  • Pyruvate Dehydrogenase Acetyl-Transferring Kinase / antagonists & inhibitors
  • Signal Transduction / drug effects
  • Squamous Cell Carcinoma of Head and Neck* / drug therapy
  • Xenograft Model Antitumor Assays

Substances

  • Antineoplastic Agents
  • Polymers
  • Proto-Oncogene Proteins c-akt
  • Drug Carriers
  • ErbB Receptors
  • Pyruvate Dehydrogenase Acetyl-Transferring Kinase
  • Phosphoinositide-3 Kinase Inhibitors

Grants and funding

This work was supported by the Universidad Europea de Madrid under Grant [2017/UEM21 and 2019/UEM06].