A fully contained sample holder capable of electron-yield detection at soft X-ray energies

J Synchrotron Radiat. 2025 Jan 1. doi: 10.1107/S1600577524011354. Online ahead of print.

Abstract

A holder has been developed that enables electron yield-detected soft X-ray spectroscopy of fully contained samples at low temperature. Crucially, this design uses elements of the sample containment to collect ejected electrons, removing the need to expose samples directly to the vacuum environment of the spectrometer. The design is modular and should be adaptable to a number of different endstation configurations, enabling spectroscopy of air-sensitive, radioactive and vacuum-sensitive (biological) samples.

Keywords: X-ray magnetic circular dichroism; XAS; XMCD; holders; soft X-ray absorption spectroscopy; soft X-rays; total electron yield.