GingisREX: A Complementary Enzyme for the Detection of Bacterial Proteins

J Am Soc Mass Spectrom. 2024 Dec 4;35(12):2790-2794. doi: 10.1021/jasms.4c00347. Epub 2024 Oct 11.

Abstract

Reliable enzymatic digestion underscores successful mass-spectrometry-based proteomics experiments. In this study, we compare the use of the arginine-specific protease, GingisREX, against a more traditional approach in the identification of Escherichia coli proteins. An increased number of protein identifications were noted when GingisREX was used compared to a trypsin/lys-C mixture. This improvement was attributed to the generation of fewer peptides per protein, resulting in a simpler peptide mixture. Furthermore, GingisREX exhibited increased digestion efficiency, fewer missed cleavages, and improved MS/MS data quality for higher molecular weight peptides. The data here establish GingisREX to be a protease complementary to trypsin for enhanced detection of bacterial proteins. With further optimization, GingisREX could prove to be an effective alternative to trypsin for identifying host cell proteins in biotherapeutics.

MeSH terms

  • Escherichia coli Proteins* / analysis
  • Escherichia coli Proteins* / chemistry
  • Escherichia coli Proteins* / metabolism
  • Escherichia coli* / chemistry
  • Escherichia coli* / enzymology
  • Proteomics* / methods
  • Tandem Mass Spectrometry* / methods
  • Trypsin* / chemistry
  • Trypsin* / metabolism

Substances

  • Escherichia coli Proteins
  • Trypsin