Phytic acid-induced durable fire-proof and hydrophobic complex coating for versatile cotton fabrics

Int J Biol Macromol. 2024 Nov;281(Pt 2):135733. doi: 10.1016/j.ijbiomac.2024.135733. Epub 2024 Sep 30.

Abstract

To address the current development requirements for multifunctional cotton fabrics, a phytic acid-induced flame-retardant hydrophobic coating containing nitrogen (N), phosphorus (P), and silicon (Si) was grafted on the surface of cotton fabrics using a facile step-by-step immersion method. The limiting oxygen index value improved to 31.2 %, decreasing to 26.7 % after 50 laundering cycles, while the fabric remained self-extinguishing effect in the vertical flammability test and showed a water contact angle of 126.1°. Cone calorimetry test showed that the modified fabric could not be ignited at the irradiation heat flux of 35 kW/m2. When the irradiation heat flux was raised to 50 kW/m2, there was a significant decline in the peak heat release rate of the modified cotton fabric, which decreased by 43.2 % to a remarkably low value of 114.0 kW/m2, indicating excellent flame-retardant properties. The analysis of the flame-retardant mechanism uncovered that the modified coating exhibited a significant dual flame-retardant mechanism involving both the gaseous phase and the condensed phase. Additionally, the oil-water separation tests revealed that the separation efficiency of the modified cotton fabrics was as high as 97.1 % and remained around 96 % after 10 cycles, which made them reusable for the clean-up of hazardous chemicals.

Keywords: Hydrophobicity; Poly (phytic acid-co-polyethyleneimine); Self-extinguishing effect.

MeSH terms

  • Cotton Fiber*
  • Fires
  • Flame Retardants
  • Hydrophobic and Hydrophilic Interactions*
  • Nitrogen / chemistry
  • Phosphorus / chemistry
  • Phytic Acid* / chemistry
  • Textiles

Substances

  • Phytic Acid
  • Flame Retardants
  • Nitrogen
  • Phosphorus