Pd(II)-Catalyzed C4-Selective Alkynylation of Indoles by a Transient Directing Group

Org Lett. 2024 Aug 16;26(32):6819-6824. doi: 10.1021/acs.orglett.4c01970. Epub 2024 Aug 6.

Abstract

With alanine as a transient directing group, Pd-catalyzed regioselective alkynylation at the indole C4-position was successfully established in a good yield. The total synthesis of the PAF antagonist demonstrated the synthetic utility of this protocol. The regioselectivity was explicitly proven by the prepared C4-selective palladacycle intermediate in the catalytic process and the DFT calculation of the energy barriers of C4- and C2-site-selective C-H activation of indole.