Uncommon Epoxyquinols Pyrrolocytosporin A and Cytosporin E2 from the Fungus Eutypella sp. D-1

Chem Biodivers. 2024 Aug;21(8):e202401097. doi: 10.1002/cbdv.202401097. Epub 2024 Jun 28.

Abstract

Two uncommon epoxyquinols, pyrrolocytosporin A (1) and cytosporin E2 (2), along with the known cytosporin Y1 (3), were isolated from the solid defined medium of the Arctic-derived fungus Eutypella sp. D-1. Their structures were established through comprehensive analyses of spectroscopic and electronic circular dichroism data. Structurally, compound 1 represented the first nitrogen-containing epoxyquinol characterized by a pyrrole fused cytosporin framework, while compound 2 contained an uncommon cyclic carbonate functionality. The antibacterial, immunosuppressive, anti-inflammatory, and cytotoxic activities of all compounds were evaluated. Among the three metabolites, only compound 1 exhibited inhibitory effects on nitric oxide production induced by lipopolysaccharide with an IC50 value of 6.55 μM. Additionally, only compound 2 displayed inhibitory activity against ConA-induced T-cell proliferation with an IC50 value of 9.85 μM.

Keywords: Anti-inflammatory activity; Cytosporin; Epoxyquinol; Eutypella sp. D-1; Immunosuppressive activity.

MeSH terms

  • Animals
  • Anti-Bacterial Agents / chemistry
  • Anti-Bacterial Agents / isolation & purification
  • Anti-Bacterial Agents / pharmacology
  • Antineoplastic Agents / chemistry
  • Antineoplastic Agents / isolation & purification
  • Antineoplastic Agents / pharmacology
  • Cell Proliferation* / drug effects
  • Dose-Response Relationship, Drug
  • Humans
  • Lipopolysaccharides* / antagonists & inhibitors
  • Lipopolysaccharides* / pharmacology
  • Mice
  • Microbial Sensitivity Tests
  • Molecular Conformation
  • Molecular Structure
  • Nitric Oxide* / antagonists & inhibitors
  • Nitric Oxide* / biosynthesis
  • Nitric Oxide* / metabolism
  • Pyrroles / chemistry
  • Pyrroles / isolation & purification
  • Pyrroles / pharmacology
  • RAW 264.7 Cells
  • T-Lymphocytes / drug effects

Substances

  • Nitric Oxide
  • Lipopolysaccharides
  • Anti-Bacterial Agents
  • Antineoplastic Agents
  • Pyrroles