In Situ Self-Assembling Liver Spheroids with Synthetic Nanoscaffolds for Preclinical Drug Screening Applications

ACS Appl Mater Interfaces. 2024 May 22;16(20):25610-25621. doi: 10.1021/acsami.3c17384. Epub 2024 May 13.

Abstract

Drug-induced liver injury (DILI) is one of the most common reasons for acute liver failure and a major reason for the withdrawal of medications from the market. There is a growing need for advanced in vitro liver models that can effectively recapitulate hepatic function, offering a robust platform for preclinical drug screening applications. Here, we explore the potential of self-assembling liver spheroids in the presence of electrospun and cryomilled poly(caprolactone) (PCL) nanoscaffolds for use as a new preclinical drug screening tool. This study investigated the extent to which nanoscaffold concentration may have on spheroid size and viability and liver-specific biofunctionality. The efficacy of our model was further validated using a comprehensive dose-dependent acetaminophen toxicity protocol. Our findings show the strong potential of PCL-based nanoscaffolds to facilitate in situ self-assembly of liver spheroids with sizes under 350 μm. The presence of the PCL-based nanoscaffolds (0.005 and 0.01% w/v) improved spheroid viability and the secretion of critical liver-specific biomarkers, namely, albumin and urea. Liver spheroids with nanoscaffolds showed improved drug-metabolizing enzyme activity and greater sensitivity to acetaminophen compared to two-dimensional monolayer cultures and scaffold-free liver spheroids. These promising findings highlight the potential of our nanoscaffold-based liver spheroids as an in vitro liver model for drug-induced hepatotoxicity and drug screening.

Keywords: drug-induced liver injuries; liver; nanofibre; scaffolds; spheroids.

MeSH terms

  • Acetaminophen* / chemistry
  • Acetaminophen* / pharmacology
  • Animals
  • Cell Survival / drug effects
  • Chemical and Drug Induced Liver Injury / metabolism
  • Chemical and Drug Induced Liver Injury / pathology
  • Drug Evaluation, Preclinical*
  • Humans
  • Liver* / drug effects
  • Polyesters / chemistry
  • Spheroids, Cellular* / drug effects
  • Spheroids, Cellular* / metabolism
  • Tissue Scaffolds* / chemistry

Substances

  • polycaprolactone
  • Acetaminophen
  • Polyesters