Changes in the secondary structure of apolipoprotein B-100 after Cu2+-catalysed oxidation of human low-density lipoproteins monitored by Fourier transform infrared spectroscopy

Biochim Biophys Acta. 1987 Nov 21;922(2):145-54. doi: 10.1016/0005-2760(87)90148-2.

Abstract

Fourier transform infrared (FTIR) spectra have been obtained of human low-density lipoproteins (LDL) in H2O and 2H2O buffers. The absorption bands are assigned to vibrations of the lipid and apolipoprotein B-100 components. The analysis of second-derivative spectra allowed an assignment of individual protein bands to alpha-helical, random, coil or beta-structure and beta-turn conformations. Changes in the FTIR spectra after Cu2+-catalysed oxidation of the LDL particles indicate that the structure of apolipoprotein B-100 becomes less ordered, with some alterations of alpha-helical and beta-turn conformation. The main beta-structure absorption at 1620 cm-1 is unaffected by oxidation. Taking into account the resistance to oxidation and the slow H-2H exchange it is suggested that the beta-structure is hidden from external factors whereas other structures are mostly present on the surface of the LDL particle. Oxidation affects mainly the surface region of apolipoprotein B-100 and leads to a structural rearrangement which consequently changes the receptor specificity of the LDL.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Apolipoprotein B-100
  • Apolipoproteins B / blood*
  • Copper / pharmacology*
  • Fourier Analysis
  • Humans
  • Lipoproteins, LDL / blood*
  • Oxidation-Reduction
  • Protein Conformation
  • Spectrophotometry, Infrared

Substances

  • Apolipoprotein B-100
  • Apolipoproteins B
  • Lipoproteins, LDL
  • Copper