1D and 2D NMR datasets, resonance assignments and coupling constant analysis of red beet fiber and pectin

Gary D Strahan; Arland T Hotchkiss; Senghane Dieng; Julie Hirsch

doi:10.1016/j.dib.2022.108845

1D and 2D NMR datasets, resonance assignments and coupling constant analysis of red beet fiber and pectin

Data Brief. 2022 Dec 20:46:108845. doi: 10.1016/j.dib.2022.108845. eCollection 2023 Feb.

Authors

Gary D Strahan¹, Arland T Hotchkiss¹, Senghane Dieng², Julie Hirsch²

Affiliations

¹ Agricultural Research Service, U.S. Department of Agriculture, Dairy & Functional Foods Research Unit, 600 E. Mermaid Lane, Wyndmoor, PA 19038 United States of America.
² Ingredion, Inc., 10 Finderne Avenue, Bridgewater, NJ 08807 United States of America.

Abstract

The datasets presented in this article represent detailed NMR spectral analyses on red beet fiber, including the pomace, water-soluble and water-insoluble fractions, as well as the acid-extracted pectin. The samples were solvated in deuterium oxide and investigated by 1D-¹H, 1D-¹³C NMR, and multiple 2D-NMR experiments, including gCOSY, zTOCSY, HSQC, HMBC, HSQCTOCSY, and H2BC. The NMR chemical shifts, coupling constants and spin-systems were identified for the major carbohydrate residues in each sample. This article provides additional data related to the research article "Structural characterization of red beet fiber and pectin" published in Food Hydrocolloids [1].

Keywords: Fiber; NMR; Pectin; Polysaccharides; Red beet.

Published by Elsevier Inc.