Label-Free Detection of Staphylococcus aureus Based on Bacteria-Imprinted Polymer and Turn-on Fluorescence Probes

ACS Appl Bio Mater. 2021 Jan 18;4(1):420-427. doi: 10.1021/acsabm.0c00897. Epub 2020 Dec 15.

Abstract

The effective identification and quantitative determination of Staphylococcus aureus is a major public health concern. Here, an innovative strategy that combines a bacteria-imprinted polydimethylsiloxane film for bacterial recognition and fluorescence resonance energy transfer platform for turn-on fluorescence sensing is demonstrated. The bacteria-imprinted polydimethylsiloxane film was facilely fabricated to generate corresponding specific sites on the polydimethylsiloxane surface via stamp imprinting using Staphylococcus aureus as template followed by modification with 1H,1H,2H,2H-perfluorooctyltriethoxysilane. The fluorescence resonance energy transfer platform was developed through electrostatic interaction between citrate-functional copper clusters and dopamine-stabilized gold nanoparticles. When the Staphylococcus aureus are present, the 1H,1H,2H,2H-perfluorooctyltriethoxysilane-modified bacteria-imprinted polydimethylsiloxane film can precisely capture the target; subsequently, the negatively charged bacteria compete with citrate-functional copper clusters and bind to dopamine-stabilized gold nanoparticles, leading to the fluorescence recovery of citrate-functional copper clusters. The entire detection process was achieved within 135 min, showing a wide linear calibration response from 10 to 1 × 107 cfu mL-1 with a low detection limit of 11.12 cfu mL-1. Furthermore, the recoveries from spiked samples were from 97.7 to 101.90% with relative standard derivations lower than 10%. The established label-free assay of measuring Staphylococcus aureus is rapid, sensitive, specific, and efficient.

Keywords: Staphylococcus aureus; bacteria imprinted; food safety; label-free detection; turn-on fluorescence.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Citric Acid / chemistry
  • Copper / chemistry
  • Dimethylpolysiloxanes / chemistry
  • Fluorescence Resonance Energy Transfer / methods*
  • Fluorescent Dyes / chemistry*
  • Gold / chemistry
  • Limit of Detection
  • Meat / microbiology
  • Metal Nanoparticles / chemistry
  • Molecularly Imprinted Polymers / chemistry*
  • Staphylococcus aureus / isolation & purification*
  • Swine

Substances

  • Dimethylpolysiloxanes
  • Fluorescent Dyes
  • Molecularly Imprinted Polymers
  • Citric Acid
  • baysilon
  • Gold
  • Copper