Biochemical and biophysical characterization of the OXA-48-like carbapenemase OXA-436

Acta Crystallogr F Struct Biol Commun. 2021 Sep 1;77(Pt 9):312-318. doi: 10.1107/S2053230X21008645. Epub 2021 Aug 31.

Abstract

The crystal structure of the class D β-lactamase OXA-436 was solved to a resolution of 1.80 Å. Higher catalytic rates were found at higher temperatures for the clinically important antibiotic imipenem, indicating better adaptation of OXA-436 to its mesophilic host than OXA-48, which is believed to originate from an environmental source. Furthermore, based on the most populated conformations during 100 ns molecular-dynamics simulations, it is postulated that the modulation of activity involves conformational shifts of the α3-α4 and β5-β6 loops. While these changes overall do not cause clinically significant shifts in the resistance profile, they show that antibiotic-resistance enzymes exist in a continuum. It is believed that these seemingly neutral differences in the sequence exist on a path leading to significant changes in substrate selectivity.

Keywords: X-ray crystal structure; antibiotic resistance; carbapenemase OXA-436; thermostability.

MeSH terms

  • Bacterial Proteins / chemistry*
  • Bacterial Proteins / metabolism*
  • Catalytic Domain
  • Crystallography, X-Ray
  • Models, Molecular*
  • Protein Conformation
  • Shewanella putrefaciens / enzymology
  • Substrate Specificity
  • beta-Lactamases / chemistry*
  • beta-Lactamases / metabolism*

Substances

  • Bacterial Proteins
  • beta-Lactamases
  • carbapenemase