Design and biological evaluation of novel long-acting adalimumab Fab conjugated with the albumin binding domain

Eur J Pharmacol. 2021 Aug 5:904:174152. doi: 10.1016/j.ejphar.2021.174152. Epub 2021 May 5.

Abstract

Antigen-binding fragments (Fabs) are preferred alternatives to antibodies for medical application, whereas their short half-lives limit therapeutic effectiveness. Albumin binding domain (ABD) with high affinity for albumin possesses a great potential in enhancing in vivo performance of biotherapeutics. In this study, to mitigate the poor pharmacokinetics of adalimumab Fab targeting tumor necrosis factor-α (TNFα), an ABD fusion strategy was applied innovatively using GA3, ABD035, ABD094 and ABDCon with high affinities for albumin. The prokaryotic expression, bioactivities and half-lives of those novel Fab-ABD fusions were investigated in vitro and in vivo. All Fab-ABD fusions were successfully purified, and they retained similar TNFα-binding activities with the unmodified Fab control, also presented high affinities for human/mouse serum albumin (HSA/MSA). Additionally, the simultaneous binding of the difunctional Fab-ABD fusions to TNFα and albumin was verified, and ABD fused to Fab neither interfered with Fab-TNFα binding nor impaired the association between Fc fragment of IgG receptor and transporter (FcRn) and albumin. Based on the highest binding affinity for HSA and maximal yield, Fab-ABDCon was selected for further evaluation. Fab-ABDCon showed similar thermostability with the Fab control and robust stability in human and mouse plasma. Most notably, the pharmacokinetics of Fab-ABDCon in mice was significantly improved with a 22-fold longer plasma half-life (28.2 h) compared with that of Fab control (1.31 h), which have contributed to its satisfactory therapeutic efficacy in murine TNFα-induced hepatonecrosis model. Thus, Fab-ABDCon could be a promising long-acting candidate suitable for drug development targeting TNFα-mediated inflammatory disease.

Keywords: Adalimumab; Albumin binding domain; Fab fragment; Half-life; Pharmacokinetics; TNFα.

MeSH terms

  • Adalimumab / biosynthesis*
  • Adalimumab / pharmacology*
  • Albumins / immunology
  • Albumins / metabolism*
  • Animals
  • Anti-Inflammatory Agents / immunology
  • Anti-Inflammatory Agents / pharmacology*
  • Cell Death / drug effects
  • Cell Line, Tumor
  • Chemical and Drug Induced Liver Injury / prevention & control
  • Drug Design
  • Female
  • Galactosamine / administration & dosage
  • Galactosamine / toxicity
  • Half-Life
  • Humans
  • Hydrogen-Ion Concentration
  • Immunoglobulin Fab Fragments / biosynthesis*
  • Immunoglobulin Fab Fragments / pharmacology
  • Injections, Intraperitoneal
  • Mice
  • Mice, Inbred BALB C
  • Necrosis / chemically induced
  • Necrosis / prevention & control
  • Protein Binding / genetics
  • Protein Domains / genetics
  • Receptors, Fc / immunology
  • Receptors, Fc / metabolism
  • Recombinant Fusion Proteins / administration & dosage
  • Recombinant Fusion Proteins / biosynthesis*
  • Recombinant Fusion Proteins / immunology
  • Recombinant Fusion Proteins / pharmacology*
  • Serum Albumin, Human / immunology
  • Serum Albumin, Human / metabolism
  • Tumor Necrosis Factor-alpha / administration & dosage
  • Tumor Necrosis Factor-alpha / antagonists & inhibitors
  • Tumor Necrosis Factor-alpha / immunology
  • Tumor Necrosis Factor-alpha / toxicity

Substances

  • Albumins
  • Anti-Inflammatory Agents
  • Immunoglobulin Fab Fragments
  • Receptors, Fc
  • Recombinant Fusion Proteins
  • Tumor Necrosis Factor-alpha
  • Galactosamine
  • Adalimumab
  • Serum Albumin, Human