Extraction and characterization of starch from Yard-long bean (Vigna unguiculata (L.) Walp. ssp. unguiculata cv.-gr. sesquipedalis)

Int J Biol Macromol. 2021 Jun 30:181:1023-1029. doi: 10.1016/j.ijbiomac.2021.04.127. Epub 2021 Apr 21.

Abstract

Vigna unguiculata subsp. sesquipedalis is an important derivative cultivar of cowpea planted widely in China, and popularly known as "Yard-long bean". There is lack of research about the structural characterization and physicochemical aspects of carbohydrate content in Yard-long bean seeds. Thus, the present study aimed to evaluate structures, thermal and technological properties of Yard-long bean seeds starch (YSS). The starch contains little of ash, protein and total fiber meanwhile amylose content of 37.52%. The shapes of the starch granules obtained from field emission scanning electron microscopy (FESEM) were oval to semi-elliptical with little granules occurring in agglomerated structures clusters, and volume median diameter of granules ranged from 10.5 μm to 12.5 μm. The initial gelatinization temperature of YSS was 73.86 °C, peak temperature was 80.59 °C and final 88.53 °C. Solubility index (SI, 3.43% at 90 °C) and swelling power (SP, 6.62 g/g at 90 °C) were observed with low volume, which corroborated with the C-type structure shown by X-ray diffraction (XRD) and high crystallinity degree. The extraction of YSS can be feasible, and it has suitable properties for use in the food industry.

Keywords: Cowpea; Granule structure; Physicochemical properties; Starch; Yard-long bean.

MeSH terms

  • Amylose / chemistry*
  • China
  • Dietary Fiber*
  • Seeds / chemistry
  • Solubility
  • Starch / chemistry*
  • Starch / isolation & purification
  • Temperature
  • Vigna / chemistry*
  • X-Ray Diffraction

Substances

  • Dietary Fiber
  • Starch
  • Amylose