High Affinity of Chlorin e6 to Immunoglobulin G for Intraoperative Fluorescence Image-Guided Cancer Photodynamic and Checkpoint Blockade Therapy

ACS Nano. 2019 Sep 24;13(9):10242-10260. doi: 10.1021/acsnano.9b03466. Epub 2019 Aug 19.

Abstract

Cancer photodynamic therapy (PDT) represents an attractive local treatment in combination with immunotherapy. Successful cancer PDT relies on image guidance to ensure the treatment accuracy. However, existing nanotechnology for co-delivery of photosensitizers and image contrast agents slows the clearance of PDT agents from the body and causes a disparity between the release profiles of the imaging and PDT agents. We have found that the photosensitizer Chlorin e6 (Ce6) is inherently bound to immunoglobulin G (IgG) in a nanomolarity range of affinity. Ce6 and IgG self-assemble to form the nanocomplexes termed Chloringlobulin (Chlorin e6 + immunoglobulin G). Chloringlobulin enhances the Ce6 concentration in the tumor without changing its elimination half-life in blood. Utilizing the immune checkpoint inhibitor antiprogrammed death ligand 1 (PD-L1) (αPD-L1) to prepare αPD-L1 Chloringlobulin, we have demonstrated a combination of Ce6-based red-light fluorescence image-guided surgery, stereotactic PDT, and PD-L1 blockade therapy of mice bearing orthotopic glioma. In mice bearing an orthotopic colon cancer model, we have prepared another Chloringlobulin that allows intraoperative fluorescence image-guided PDT in combination with PD-L1 and cytotoxic T lymphocyte antigen 4 (CTLA-4) dual checkpoint blockade therapy. The Chloringlobulin technology shows great potential for clinical translation of combinatorial intraoperative fluorescence image-guided PDT and checkpoint blockade therapy.

Keywords: Chlorin e6; cytotoxic T-lymphocyte-associated antigen 4; fluorescence image-guided surgery; immunoglobulin G; photodynamic therapy; programmed death ligand 1.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • B7-H1 Antigen / antagonists & inhibitors
  • B7-H1 Antigen / metabolism
  • CTLA-4 Antigen / antagonists & inhibitors
  • CTLA-4 Antigen / metabolism
  • Cell Line, Tumor
  • Chlorophyllides
  • Female
  • Fluorescence
  • Immunoglobulin G / metabolism*
  • Immunotherapy*
  • Intraoperative Care*
  • Male
  • Mice, Inbred BALB C
  • Mice, Inbred C57BL
  • Neoplasms / surgery
  • Neoplasms / therapy*
  • Photochemotherapy*
  • Porphyrins / chemistry*
  • Porphyrins / pharmacokinetics
  • Rats
  • Tissue Distribution

Substances

  • B7-H1 Antigen
  • CTLA-4 Antigen
  • Chlorophyllides
  • Immunoglobulin G
  • Porphyrins
  • phytochlorin