Synthesis of a magnetic polystyrene-based cation-exchange resin and its utilization for the efficient removal of cadmium (II)

Water Sci Technol. 2018 Jul;2017(3):770-781. doi: 10.2166/wst.2018.239.

Abstract

A magnetic cation-exchange resin (MCER) was prepared by copolymerization of oleic acid-grafted magnetite with styrene, divinylbenzene (DVB), and triallylisocyanurate (TAIC) for removing Cd(II) from wastewater. A non-magnetic cation-exchange polystyrene resin (CEPR) was also prepared as a reference. Structural and morphological analyses revealed that the MCER and CEPR were mesoporous microspheres; the MCER contained about 25% Fe3O4. The influence of temperature, pH, contact time, and the initial concentration of Cd(II) on the adsorption of Cd(II) was investigated. The maximum adsorption capacity of the MCER reached 88.56 mg/g, which was achieved at 343 K using a Cd(II) initial concentration of 200 mg/L. The adsorption processes attained equilibrium within 120 min for the MCER and 300 min for the CEPR, and were well described by a pseudo-second-order kinetic model. Furthermore, the equilibrium adsorption data fitted the Freundlich isotherm model better than the Langmuir model. The superior magnetic response and regeneration of the MCER make it a good candidate as an adsorbent for removing Cd(II) from wastewater.

MeSH terms

  • Adsorption
  • Cadmium / chemistry*
  • Cation Exchange Resins / chemistry*
  • Cations / analysis
  • Ferrosoferric Oxide
  • Hydrogen-Ion Concentration
  • Kinetics
  • Polystyrenes / chemistry*
  • Temperature
  • Wastewater / chemistry*
  • Water Pollutants, Chemical / chemistry*
  • Water Purification / methods

Substances

  • Cation Exchange Resins
  • Cations
  • Polystyrenes
  • Waste Water
  • Water Pollutants, Chemical
  • Cadmium
  • Ferrosoferric Oxide