Both glypican-3/Wnt/β-catenin signaling pathway and autophagy contributed to the inhibitory effect of curcumin on hepatocellular carcinoma

Dig Liver Dis. 2019 Jan;51(1):120-126. doi: 10.1016/j.dld.2018.06.012. Epub 2018 Jun 21.

Abstract

Aim: The aim of this study is to investigate the role of glypican-3(GPC3)/wnt/β-catenin signaling pathway and autophagy in the regulation of hepatocellular carcinoma (HCC) growth mediated by curcumin.

Methods: HepG2 cells were treated with various concentrations of curcumin and/or GPC3-targeting siRNA in the presence or absence of 3-MA. Cell proliferation and apoptosis were determined by MTT and TUNEL assay, respectively. Expression of GPC3, β-catenin, c-myc, LC3, and Beclin1 was determined by western blotting. In addition, curcumin was tested in tumor xenografts mice model, Caliper IVIS Lumina II was used to monitor the tumor growth, and GPC3/wnt/β-catenin signaling proteins were determined by western blotting.

Results: Curcumin treatment led to proliferation inhibition and apoptosis induction in HepG2 cells in a concentration-dependent manner, and suppressed HCC tumor growth in vivo. Further analysis showed that curcumin treatment inactivated Wnt/β-catenin signaling and decreased GPC3 expression, silencing of GPC3 expression promoted the effects of curcumin on Wnt/β-catenin signaling. In addition, inhibiting autophagy by 3-MA relieved curcumin-dependent down-regulation of GPC3.

Conclusion: Curcumin suppressed HCC tumor growth through down-regulating GPC3/wnt/β-catenin signaling pathway, which was partially mediated by activation of autophagy.

Keywords: Apoptosis; Curcumin; Glypican-3; HepG2; Hepatocellular carcinoma; Wnt/β-catenin.

MeSH terms

  • Animals
  • Apoptosis / drug effects
  • Blotting, Western
  • Carcinoma, Hepatocellular / enzymology
  • Carcinoma, Hepatocellular / genetics*
  • Cell Proliferation / drug effects
  • Curcumin / administration & dosage
  • Curcumin / pharmacology*
  • Down-Regulation
  • Gene Expression Regulation, Neoplastic
  • Glypicans / metabolism*
  • Hep G2 Cells / metabolism
  • Humans
  • Liver Neoplasms / enzymology
  • Liver Neoplasms / genetics*
  • Mice
  • Mice, Nude
  • Real-Time Polymerase Chain Reaction
  • Wnt3 Protein
  • beta Catenin / metabolism

Substances

  • CTNNB1 protein, human
  • GPC3 protein, human
  • Glypicans
  • Wnt3 Protein
  • beta Catenin
  • Curcumin