Cyclization of Ketones with Nitriles under Base: A General and Economical Synthesis of Pyrimidines

Org Lett. 2018 Jun 1;20(11):3399-3402. doi: 10.1021/acs.orglett.8b01324. Epub 2018 May 23.

Abstract

A facile, general, and economical synthesis of diversely functionalized pyrimidines has been realized under basic conditions via the copper-catalyzed cyclization of ketones with nitriles. The reaction proceeds via a novel pathway involving the nitriles acting as electrophiles and consecutive C-C bond and two C-N bond formations and shows broad substrate scope and good tolerance of many important functional groups. This strategy represents a new platform for constructing pyrimidine structures.

Publication types

  • Research Support, Non-U.S. Gov't