A rapid fluorogenic GPCR-β-arrestin interaction assay

Protein Sci. 2018 Apr;27(4):874-879. doi: 10.1002/pro.3385. Epub 2018 Feb 23.

Abstract

Detection of protein-protein interactions involved in signal transduction in live cells and organisms has a variety of important applications. We report a fluorogenic assay for G protein-coupled receptor (GPCR)-β-arrestin interaction that is genetically encoded, generalizes to multiple GPCRs, and features high signal-to-noise because fluorescence is absent until its components interact upon GPCR activation. Fluorescence after protease-activated receptor-1 activation developed in minutes and required specific serine-threonine residues in the receptor carboxyl tail, consistent with a classical G protein-coupled receptor kinase dependent β-arrestin recruitment mechanism. This assay provides a useful complement to other in vivo assays of GPCR activation.

Keywords: G protein coupled receptor; fluorescent reporter; green fluorescent protein; protein-protein interaction.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Green Fluorescent Proteins / genetics
  • Green Fluorescent Proteins / metabolism
  • HEK293 Cells
  • Humans
  • Microscopy, Confocal
  • Mutation
  • Protein Interaction Mapping / methods*
  • Receptor, PAR-1 / genetics
  • Receptor, PAR-1 / metabolism
  • Receptor, PAR-2 / genetics
  • Receptor, PAR-2 / metabolism
  • Receptors, G-Protein-Coupled / genetics
  • Receptors, G-Protein-Coupled / metabolism*
  • Recombinant Proteins / genetics
  • Recombinant Proteins / metabolism
  • Signal-To-Noise Ratio
  • Time-Lapse Imaging / methods
  • beta-Arrestins / genetics
  • beta-Arrestins / metabolism*

Substances

  • Receptor, PAR-1
  • Receptor, PAR-2
  • Receptors, G-Protein-Coupled
  • Recombinant Proteins
  • beta-Arrestins
  • Green Fluorescent Proteins