Atomic-resolution structures from fragmented protein crystals with the cryoEM method MicroED

Nat Methods. 2017 Feb 13;14(4):399-402. doi: 10.1038/nmeth.4178.

Abstract

Traditionally, crystallographic analysis of macromolecules has depended on large, well-ordered crystals, which often require significant effort to obtain. Even sizable crystals sometimes suffer from pathologies that render them inappropriate for high-resolution structure determination. Here we show that fragmentation of large, imperfect crystals into microcrystals or nanocrystals can provide a simple path for high-resolution structure determination by the cryoEM method MicroED and potentially by serial femtosecond crystallography.

MeSH terms

  • Cryoelectron Microscopy / methods*
  • Crystallography / methods*
  • Crystallography, X-Ray / methods
  • Models, Molecular
  • Protein Conformation
  • Proteins / chemistry*

Substances

  • Proteins