The A2b adenosine receptor antagonist PSB-603 promotes oxidative phosphorylation and ROS production in colorectal cancer cells via adenosine receptor-independent mechanism

Cancer Lett. 2016 Dec 1;383(1):135-143. doi: 10.1016/j.canlet.2016.09.018. Epub 2016 Sep 28.

Abstract

Purpose: Adenosine is a multifaceted regulator of tumor progression. It modulates immune cell activity as well as acting directly on tumor cells. The A2b adenosine receptor (A2b-AR) is thought to be an important mediator of these effects. In this study we sought to analyze the contribution of the A2b-AR to the behavior of colorectal cancer cells.

Principal results: The A2b-AR antagonist PSB-603 changed cellular redox state without affecting cellular viability. Quantification of cellular bioenergetics demonstrated that PSB-603 increased basal oxygen consumption rates, indicative of enhanced mitochondrial oxidative phosphorylation. Unexpectedly, pharmacological and genetic approaches to antagonize AR-related signalling of PSB-603 did not abolish the response, suggesting that it was AR-independent. PSB-603 also induced acute increases in reactive oxygen species, and PSB-603 synergized with chemotherapy treatment to increase colorectal cancer cell death, consistent with the known link between cellular metabolism and chemotherapy response.

Major conclusions: PSB-603 alters cellular metabolism in colorectal cancer cells and increases their sensitivity to chemotherapy. Although requiring more mechanistic insight into its A2b-AR-independent activity, our results show that PSB-603 may have clinical value as an anti-colorectal cancer therapeutic.

Keywords: Cellular redox state; Chemotherapy; MTT; Off-target effect; PSB603; Reactive oxygen species.

MeSH terms

  • Adenosine A2 Receptor Antagonists / pharmacology*
  • Antineoplastic Agents / pharmacology*
  • Antineoplastic Combined Chemotherapy Protocols / pharmacology
  • Cell Death / drug effects
  • Cell Line, Tumor
  • Colorectal Neoplasms / drug therapy*
  • Colorectal Neoplasms / genetics
  • Colorectal Neoplasms / metabolism
  • Colorectal Neoplasms / pathology
  • Cyclic AMP / metabolism
  • Dose-Response Relationship, Drug
  • Endocytosis / drug effects
  • Fluorouracil / pharmacology
  • Humans
  • Mitochondria / drug effects*
  • Mitochondria / metabolism
  • Organoplatinum Compounds / pharmacology
  • Oxaliplatin
  • Oxidation-Reduction
  • Oxidative Phosphorylation / drug effects*
  • Oxidative Stress / drug effects*
  • Oxygen Consumption / drug effects
  • RNA Interference
  • Reactive Oxygen Species / metabolism*
  • Receptor, Adenosine A2B / drug effects*
  • Receptor, Adenosine A2B / genetics
  • Receptor, Adenosine A2B / metabolism
  • Signal Transduction / drug effects
  • Sulfonamides / pharmacology*
  • Time Factors
  • Transfection
  • Xanthines / pharmacology*

Substances

  • Adenosine A2 Receptor Antagonists
  • Antineoplastic Agents
  • Organoplatinum Compounds
  • PSB603
  • Reactive Oxygen Species
  • Receptor, Adenosine A2B
  • Sulfonamides
  • Xanthines
  • Oxaliplatin
  • Cyclic AMP
  • Fluorouracil