Urinary NMR-based metabolomic analysis of rats possessing variable sperm count following orally administered Eurycoma longifolia extracts of different quassinoid levels

J Ethnopharmacol. 2016 Apr 22:182:80-9. doi: 10.1016/j.jep.2016.02.015. Epub 2016 Feb 16.

Abstract

Ethnopharmacological relevance: Eurycoma longifolia (Tongkat Ali, TA) roots have been ethnically used as a remedy to boost male sexual desire, libido, energy and fertility.

Aim of the study: The study evaluated the effect of TA extracts with different quassinoid levels on rats sperm count and examined corresponding post-treatment urinary metabolic changes.

Materials and methods: Twenty-four male Sprague-Dawley rats, categorized into 4 groups of 6 rats each, were orally administered for 48 days with water for the control (group 1), 125mg/kg of TA water extract (TAW, group 2), 125mg/kg of TA quassinoid-poor extract (TAQP, group 3) and 21mg/kg of TA quassinoid-rich extract (TAQR, group 4). Upon completion of the 48-day treatment, the urine samples were analyzed by NMR and the animals were subsequently sacrificed for sperm count analysis. The urine profiles were categorized according to sperm count level.

Results: The results showed that the sperm count in TAW- and TAQR-treated groups was significantly higher compared to the TAQP-administered and control groups. The orthogonal partial least squares discriminant analysis (OPLS-DA) model indicated a clear separation among the urine profiles with respect to sperm count level. Urine (1)H-NMR profiles of the high-sperm count group contained higher concentrations of trigonelline, alanine, benzoic acid and higher intensity of a signal at 3.42ppm, while ethanol was at higher concentration in the normal-sperm count group.

Conclusions: The results proved the efficacy of quassinoids on sperm count increase in rats and provided quantitative markers in urine suitable for analysis of sperm profile and male fertility status.

Keywords: Eurycoma longifolia; NMR-based metabolomics; Quassinoids; Rat sperm count; Urine.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Administration, Oral
  • Alanine / urine
  • Alkaloids / urine
  • Animals
  • Benzoic Acid / urine
  • Biomarkers / urine
  • Ethanol / urine
  • Eurycoma*
  • Male
  • Metabolomics*
  • Plant Extracts / pharmacology*
  • Proton Magnetic Resonance Spectroscopy
  • Rats
  • Rats, Sprague-Dawley
  • Sperm Count*

Substances

  • Alkaloids
  • Biomarkers
  • Plant Extracts
  • Ethanol
  • trigonelline
  • Benzoic Acid
  • Alanine