Long-range interaction between the Mn4CaO5 cluster and the non-heme iron center in photosystem II as revealed by FTIR spectroelectrochemistry

Biochemistry. 2014 Aug 5;53(30):4914-23. doi: 10.1021/bi500549b. Epub 2014 Jul 25.

Abstract

It is known that inactivation of the Mn4CaO5 cluster, the catalytic center of water oxidation in photosystem II (PSII), induces a positive shift of the redox potential (Em) of the primary quinone electron acceptor QA by ∼+150 mV, resulting in suppression of the electron transfer from QA to the secondary quinone acceptor QB. Although the relevance of this Em(QA(-)/QA) shift to the photoprotection of PSII has been debated, its molecular mechanism is still enigmatic from a structural viewpoint because QA is ∼40 Å from the Mn4CaO5 cluster. In this work, we have investigated the influence of Mn depletion on the Em of the non-heme iron, which is located between QA and QB, and its surrounding structure. Electrochemical measurements in combination with Fourier transform infrared (FTIR) spectroscopy revealed that Mn depletion shifts Em(Fe(2+)/Fe(3+)) by +18 mV, which is ∼8 times smaller than the shift of Em(QA(-)/QA). Comparison of the Fe(2+)/Fe(3+) FTIR difference spectra between intact and Mn-depleted PSII samples showed that Mn depletion altered the pKa's of a His ligand to the non-heme iron, most probably the D1-His215 interacting QB, and a carboxylate group, possibly D1-Glu244, coupled with the non-heme iron. It was further shown that Mn depletion influences the C≡N vibration of bromoxynil bound to the QB site, indicative of the modification of the QB binding site. On the basis of these results, we discuss the mechanism of a long-range interaction between the donor and acceptor sides of PSII.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Binding Sites / physiology
  • Calcium Compounds / chemistry
  • Calcium Compounds / metabolism*
  • Crystallography, X-Ray
  • Electrochemical Techniques / methods*
  • Manganese Compounds / chemistry
  • Manganese Compounds / metabolism*
  • Oxides / chemistry
  • Oxides / metabolism*
  • Photosystem II Protein Complex / chemistry
  • Photosystem II Protein Complex / metabolism*
  • Spectroscopy, Fourier Transform Infrared / methods

Substances

  • Calcium Compounds
  • Manganese Compounds
  • Oxides
  • Photosystem II Protein Complex
  • lime