Identification of promiscuous ene-reductase activity by mining structural databases using active site constellations

Nat Commun. 2014 Jun 23:5:4150. doi: 10.1038/ncomms5150.

Abstract

The exploitation of catalytic promiscuity and the application of de novo design have recently opened the access to novel, non-natural enzymatic activities. Here we describe a structural bioinformatic method for predicting catalytic activities of enzymes based on three-dimensional constellations of functional groups in active sites ('catalophores'). As a proof-of-concept we identify two enzymes with predicted promiscuous ene-reductase activity (reduction of activated C-C double bonds) and compare them with known ene-reductases, that is, members of the Old Yellow Enzyme family. Despite completely different amino acid sequences, overall structures and protein folds, high-resolution crystal structures reveal equivalent binding modes of typical Old Yellow Enzyme substrates and ligands. Biochemical and biocatalytic data show that the two enzymes indeed possess ene-reductase activity and reveal an inverted stereopreference compared with Old Yellow Enzymes for some substrates. This method could thus be a tool for the identification of viable starting points for the development and engineering of novel biocatalysts.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Proteins / chemistry*
  • Bacterial Proteins / genetics
  • Bacterial Proteins / metabolism*
  • Catalysis
  • Catalytic Domain
  • Crystallography, X-Ray
  • Databases, Protein
  • Kinetics
  • Models, Molecular
  • Oxidoreductases / chemistry*
  • Oxidoreductases / genetics
  • Oxidoreductases / metabolism*
  • Protein Conformation
  • Thermus thermophilus / chemistry
  • Thermus thermophilus / enzymology*
  • Thermus thermophilus / genetics

Substances

  • Bacterial Proteins
  • Oxidoreductases

Associated data

  • PDB/3ZOC
  • PDB/3ZOD
  • PDB/3ZOE
  • PDB/3ZOF
  • PDB/3ZOG
  • PDB/3ZOH