A structural and biochemical model of processive chitin synthesis

J Biol Chem. 2014 Aug 15;289(33):23020-23028. doi: 10.1074/jbc.M114.563353. Epub 2014 Jun 18.

Abstract

Chitin synthases (CHS) produce chitin, an essential component of the fungal cell wall. The molecular mechanism of processive chitin synthesis is not understood, limiting the discovery of new inhibitors of this enzyme class. We identified the bacterial glycosyltransferase NodC as an appropriate model system to study the general structure and reaction mechanism of CHS. A high throughput screening-compatible novel assay demonstrates that a known inhibitor of fungal CHS also inhibit NodC. A structural model of NodC, on the basis of the recently published BcsA cellulose synthase structure, enabled probing of the catalytic mechanism by mutagenesis, demonstrating the essential roles of the DD and QXXRW catalytic motifs. The NodC membrane topology was mapped, validating the structural model. Together, these approaches give insight into the CHS structure and mechanism and provide a platform for the discovery of inhibitors for this antifungal target.

Keywords: Carbohydrate Biosynthesis; Enzyme Inhibitor; Enzyme Mechanism; Glycosyltransferase; Protein Structure.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Motifs
  • Bacterial Proteins* / chemistry
  • Bacterial Proteins* / metabolism
  • Chitin Synthase* / chemistry
  • Chitin Synthase* / metabolism
  • Chitin* / biosynthesis
  • Chitin* / chemistry
  • Glucosyltransferases / chemistry
  • Glucosyltransferases / metabolism
  • Models, Biological*
  • Models, Molecular*
  • Sinorhizobium meliloti / enzymology*

Substances

  • Bacterial Proteins
  • Chitin
  • Glucosyltransferases
  • cellulose synthase
  • Chitin Synthase