Improvement of pulmonary absorptions of poorly absorbable drugs using Gelucire 44/14 as an absorption enhancer

J Pharm Pharmacol. 2014 Oct;66(10):1410-20. doi: 10.1111/jphp.12274. Epub 2014 May 22.

Abstract

Objectives: This study aims to evaluate the absorption-enhancing effects of Gelucire 44/14 on the pulmonary absorption of different poorly absorbable drugs and relative mechanism of action.

Methods: Absorption-enhancing effect of Gelucire 44/14 were examined by an in-vivo pulmonary absorption experiment in rats, and the membrane toxicity of Gelucire 44/14 was evaluated by measuring levels of protein and dehydrogenase (LDH) in the bronchoalveolar lavage fluid (BALF) and morphological observation.

Key findings: Pulmonary absorptions of fluorescein isothiocyanate-dextrans, insulin and calcitonin were enhanced by Gelucire 44/14 (0.1-2.0%, w/v) in a concentration-dependent manner, and the maximal absorption-enhancing effect was obtained when the concentration of Gelucire 44/14 increased to 2.0% (w/v). Furthermore, Gelucire 44/14 neither increase the levels of protein and LDH in BALF nor change morphology of lung compared with control group. In addition, a well correlation between the absorption-enhancing effect and surface tension of insulin solution in the presence of Gelucire 44/14 was observed, suggesting Gelucire 44/14-mediated decrease in the surface tension of the gas-liquid interface in alveolar tissue was possible one of the improving mechanisms of Gelucire 44/14.

Conclusion: Gelucire 44/14 was a potential and safe absorption enhancer for improving the absorption of poorly absorbable drugs including insulin and calcitonin by pulmonary delivery.

Keywords: Gelucire 44/14; absorption enhancer; membrane toxicity; poorly absorbable drugs; pulmonary absorption.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Calcitonin / chemistry
  • Calcitonin / pharmacokinetics*
  • Dextrans / pharmacokinetics*
  • Fluorescein-5-isothiocyanate / analogs & derivatives*
  • Fluorescein-5-isothiocyanate / pharmacokinetics
  • Insulin / chemistry
  • Insulin / pharmacokinetics*
  • Lung / metabolism*
  • Male
  • Pharmaceutical Preparations / chemistry
  • Polyethylene Glycols / chemistry
  • Polyethylene Glycols / pharmacology*
  • Rats, Sprague-Dawley
  • Respiratory Tract Absorption / drug effects*
  • Surface Tension

Substances

  • Dextrans
  • Insulin
  • Pharmaceutical Preparations
  • fluorescein isothiocyanate dextran
  • gelucire 44-14
  • Polyethylene Glycols
  • Calcitonin
  • Fluorescein-5-isothiocyanate