An automated synthesis-purification-sample-management platform for the accelerated generation of pharmaceutical candidates

J Lab Autom. 2014 Apr;19(2):176-82. doi: 10.1177/2211068213516325. Epub 2013 Dec 18.

Abstract

A flexible and integrated flow-chemistry-synthesis-purification compound-generation and sample-management platform has been developed to accelerate the production of small-molecule organic-compound drug candidates in pharmaceutical research. Central to the integrated system is a Mitsubishi robot, which hands off samples throughout the process to the next station, including synthesis and purification, sample dispensing for purity and quantification analysis, dry-down, and aliquot generation.

Keywords: Pharmaceutical research; automation; drug discovery; flow chemistry; high-performance liquid chromatography (HPLC); purification; synthesis.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Combinatorial Chemistry Techniques / methods*
  • Drug Discovery / methods*
  • High-Throughput Screening Assays / methods*
  • Organic Chemicals / chemical synthesis
  • Organic Chemicals / isolation & purification*
  • Organic Chemicals / pharmacology*
  • Specimen Handling / methods*

Substances

  • Organic Chemicals