Enhancing RGI lyase thermostability by targeted single point mutations

Appl Microbiol Biotechnol. 2013 Nov;97(22):9727-35. doi: 10.1007/s00253-013-5184-3. Epub 2013 Aug 31.

Abstract

Rhamnogalacturonan I lyase (RGI lyase) (EC 4.2.2.-) catalyzes the cleavage of rhamnogalacturonan I in pectins by β-elimination. In this study the thermal stability of a RGI lyase (PL 11) originating from Bacillus licheniformis DSM 13/ATCC14580 was increased by a targeted protein engineering approach involving single amino acid substitution. Nine individual amino acids were selected as targets for site-saturated mutagenesis by the use of a predictive consensus approach in combination with prediction of protein mutant stability changes and B-factor iteration testing. After extensive experimental verification of the thermal stability of the designed mutants versus the original wild-type RGI lyase, several promising single point mutations were obtained, particularly in position Glu434 on the surface of the enzyme protein. The best mutant, Glu434Leu, produced a half-life of 31 min at 60 °C, corresponding to a 1.6-fold improvement of the thermal stability compared to the original RGI lyase. Gly55Val was the second best mutation with a thermostability half-life increase of 27 min at 60 °C, and the best mutations following were Glu434Trp, Glu434Phe, and Glu434Tyr, respectively. The data verify the applicability of a combinatorial predictive approach for designing a small site saturation library for improving enzyme thermostability. In addition, new thermostable RGI lyases suitable for enzymatic upgrading of pectinaceous plant biomass materials at elevated temperatures were produced.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacillus / enzymology*
  • Bacillus / genetics
  • DNA Mutational Analysis
  • DNA, Bacterial / chemistry
  • DNA, Bacterial / genetics
  • Enzyme Stability
  • Molecular Sequence Data
  • Mutagenesis, Site-Directed
  • Mutant Proteins / chemistry
  • Mutant Proteins / genetics
  • Mutant Proteins / metabolism
  • Pectins / metabolism*
  • Point Mutation
  • Polysaccharide-Lyases / chemistry
  • Polysaccharide-Lyases / genetics*
  • Polysaccharide-Lyases / metabolism*
  • Protein Stability
  • Sequence Analysis, DNA
  • Temperature

Substances

  • DNA, Bacterial
  • Mutant Proteins
  • rhamnogalacturonan I
  • Pectins
  • Polysaccharide-Lyases

Associated data

  • GENBANK/KF373119