[Optimization of extraction process of Chrysanthemi Flos by multi-index orthogonal experiment]

Zhongguo Zhong Yao Za Zhi. 2013 Mar;38(6):821-4.
[Article in Chinese]

Abstract

Objective: To explore quantitative assessment indicators of Chrysanthemi Flos, and optimize the extraction process of Chrysanthemi Flos through orthogonal experimental design.

Method: The concentration of ethanol, amount of ethanol, extraction time and extraction frequency were selected as factors in the L9 (3(4)) orthogonal experiment. A comprehensive assessment was conducted with the peak area of the eight major common peaks in the fingerprint of Chrysanthemi Flos as the indicators.

Result: The optimum extraction process was selected as follows: using ultrasonic extraction method, adding 30-fold ethanol with 80% concentration, extracting for 2 times for extraction, 40 min for each time.

Conclusion: The optimized extraction process is reliable, with controllable assessment indicators, which is significant to the standardization of the extraction process and quality control of Chrysanthemi Flos preparations.

Publication types

  • English Abstract

MeSH terms

  • Chemical Fractionation / methods*
  • Chrysanthemum / chemistry*
  • Drugs, Chinese Herbal / chemistry
  • Drugs, Chinese Herbal / isolation & purification*
  • Ethanol / chemistry
  • Hot Temperature
  • Quality Control
  • Reproducibility of Results
  • Solubility
  • Time Factors

Substances

  • Drugs, Chinese Herbal
  • Ethanol