Pd-catalyzed C-H lactonization for expedient synthesis of biaryl lactones and total synthesis of cannabinol

Org Lett. 2013 Jun 7;15(11):2574-7. doi: 10.1021/ol400877q. Epub 2013 May 10.

Abstract

A practical Pd(II)/Pd(IV)-catalyzed carboxyl-directed C-H activation/C-O cyclization to construct biaryl lactones has been developed. The synthetic utility of this new reaction was demonstrated in an atom-economical and operationally convenient total synthesis of the natural product cannabinol from commercially available starting materials, with the newly developed method used for two key steps.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cannabinol / chemical synthesis*
  • Cannabinol / chemistry
  • Catalysis
  • Cyclization
  • Hydrogen Bonding
  • Lactones / chemical synthesis*
  • Lactones / chemistry
  • Molecular Structure
  • Palladium / chemistry*
  • Stereoisomerism

Substances

  • Lactones
  • Palladium
  • Cannabinol