Dynamic evaluation of cell surface N-glycan expression via an electrogenerated chemiluminescence biosensor based on concanavalin A-integrating gold-nanoparticle-modified Ru(bpy)3(2+)-doped silica nanoprobe

Anal Chem. 2013 May 7;85(9):4431-8. doi: 10.1021/ac303572g. Epub 2013 Apr 17.

Abstract

A sandwich electrogenerated chemiluminescence (ECL) biosensor was fabricated based on concanavalin A (Con A)-integrating gold-nanoparticle-modified Ru(bpy)3(2+)-doped silica nanoprobe (Au-RuSiO2 NPs) for in situ and dynamically evaluating cell surface N-glycan expression. Owing to the specific recognition of Con A with mannose and the core trimannoside fragment of N-glycan and the effective ECL amplification of Au-RuSiO2 NPs, the as-proposed biosensor exhibited excellent analytical performance toward the cytosensing of K562 cells with a wide detection linear range from 1.0 × 10(3) to 1.0 × 10(7) cells mL(-1) and a detection limit of 600 cells mL(-1). More importantly, the strategy was successfully applied to evaluate cell surface N-glycan expression under different external stimuli of inhibitors and enzyme. This biosensor is endowed with feasibility and reliability of generating sensitive insight into the majority of N-glycan expression on the cell surface. Furthermore, the biosensor was employed to dynamically profile cell surface N-glycan expression at different phases of cell growth in vitro. This biosensor is promising in studying and elucidating the N-glycan function in biological and physiological processes.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biosensing Techniques*
  • Cell Membrane / metabolism
  • Concanavalin A / chemistry*
  • Concanavalin A / metabolism
  • Gold / chemistry*
  • Gold / metabolism
  • Humans
  • K562 Cells
  • Luminescence*
  • Molecular Probes / chemistry
  • Nanostructures / chemistry
  • Organometallic Compounds / chemistry*
  • Organometallic Compounds / metabolism
  • Polysaccharides / biosynthesis*
  • Silicon Dioxide / chemistry
  • Silicon Dioxide / metabolism
  • Thermodynamics

Substances

  • Molecular Probes
  • Organometallic Compounds
  • Polysaccharides
  • tris(2,2'-bipyridyl)ruthenium(II)
  • Concanavalin A
  • Gold
  • Silicon Dioxide