The use of proteolysis and direct N-terminal sequence analysis to study human interleukin-2/receptor interaction on solid support

Biochem Biophys Res Commun. 1990 Jan 15;166(1):201-7. doi: 10.1016/0006-291x(90)91931-h.

Abstract

An immobilized interleukin-2 receptor which is capable of binding interleukin-2 and suitable for direct N-terminal sequence analysis was employed to study interleukin-2/receptor interactions. Sensitive tryptic sites on the immobilized receptor and its interleukin-2 complex were identified by sequence analyses and compared. The results have revealed that the N-terminal region of interleukin-2 is not involved in receptor binding and the peptide segment covering residues 36-39 in the receptor is probably near or involved in the interleukin-2 binding site. The rapidity and simplicity make this solid phase sequence approach a good method for analyzing interleukin-2/receptor interaction and may be suitable for studying other protein-ligand interactions.

MeSH terms

  • Amino Acid Sequence
  • Chromatography, Affinity / methods
  • Humans
  • Interleukin-2 / metabolism*
  • Molecular Sequence Data
  • Peptide Fragments / isolation & purification
  • Protein Conformation
  • Receptors, Interleukin-2 / metabolism*
  • Trypsin

Substances

  • Interleukin-2
  • Peptide Fragments
  • Receptors, Interleukin-2
  • Trypsin