Palladium-catalyzed regioselective [3 + 2] annulation of internal alkynes and iodo-pyranoquinolines with concomitant ring opening

Org Lett. 2012 Oct 19;14(20):5184-7. doi: 10.1021/ol3022935. Epub 2012 Sep 28.

Abstract

A regioselective tandem synthesis of highly functionalized pyrrolo[1,2-a]quinolines has been developed through a novel strategy by palladium-catalyzed [3 + 2] annulation of iodo-pyranoquinolines and internal alkynes with subsequent ring opening. Pyranoquinoline with n-alkyl substitution at the 3-position leads to the formation of pyrrolo-acridones via [3 + 2] annulations/ring opening and successive intramolecular cross-aldol condensation.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkynes / chemistry*
  • Catalysis
  • Indoles / chemistry*
  • Molecular Structure
  • Palladium / chemistry*
  • Quinolines / chemistry*

Substances

  • Alkynes
  • Indoles
  • Quinolines
  • Palladium
  • indole