Palladium(II)-catalyzed enantio- and diastereoselective synthesis of pyrrolidine derivatives

Org Lett. 2012 Aug 17;14(16):4074-7. doi: 10.1021/ol3016989. Epub 2012 Aug 8.

Abstract

A palladium-catalyzed enantio- and diastereoselective synthesis of pyrrolidine derivatives is described. Initial intramolecular nucleopalladation of the tethered protected amine forms the pyrrolidine moiety and a quinone methide intermediate. A second nucleophile adds intermolecularly to afford diverse products in high enantio- and diastereoselectivity.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Alkenes / chemistry
  • Amines / chemistry
  • Catalysis
  • Molecular Structure
  • Palladium / chemistry*
  • Pyrrolidines / chemical synthesis*
  • Pyrrolidines / chemistry
  • Stereoisomerism

Substances

  • Alkenes
  • Amines
  • Pyrrolidines
  • Palladium