A modified simple method for determination of serum α-tocopherol (vitamin E)

J Basic Clin Physiol Pharmacol. 2012 Jan 19;23(1):45-8. doi: 10.1515/jbcpp-2011-0033.

Abstract

Background: Vitamin E is one of the important antioxidants linked to regulate various diseases, such as atherosclerosis, hypertension, and male infertility. A relatively simple and economic biochemical modified method has been developed to determine serum α-tocopherol concentration.

Methods: The current modified method is based on previous Baker and Frank method and the method of Martinek by using 2,2'-bipyridyl, ferric chloride, and xylene. The complex of ferrous ions generated in this reaction with 2,2'-bipyridyl is determined by using a plain enzyme-linked immunosorbent assay microplate (non-antibody coated) at 492 nm.

Results: The standard curve of this new modified method shows a linearity with correlation r=0.997 (concentration vs. absorbance). The absorbance of this color complex is directly proportional to the α-tocopherol concentration. The sensitivity of this new modified method has been compared and correlated with Baker and Frank method by using 15 human samples (r=0.99, p<0.0001).

Conclusions: This simple and economic method may be routinely used to analyze α-tocopherol concentration in serum.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adolescent
  • Adult
  • Antioxidants / analysis*
  • Calibration
  • Enzyme-Linked Immunosorbent Assay* / standards
  • Humans
  • Middle Aged
  • Reference Standards
  • Reproducibility of Results
  • Vitamin E / blood*
  • Young Adult

Substances

  • Antioxidants
  • Vitamin E