The effects of sperminated pullulans on cornea permeability to puerarin and the toxicity

J Ocul Pharmacol Ther. 2012 Oct;28(5):497-501. doi: 10.1089/jop.2011.0263. Epub 2012 Jun 12.

Abstract

Purpose: To investigate the varied effects of sperminated pullulans (SP) with different amino residues on cornea permeability and its local toxicity.

Methods: Three groups of rabbits were used: control, low-amino residue content SP (SP-L), and high-amino residue content SP (SP-H). The in vitro and in vivo spreading assays were combined with high performance liquid chromatography (HPLC) to measure the concentration of puerarin in the external medium or aqueous humor when 0% SP, 0.2% SP-L, and 0.2% SP-H were included. The toxicity of SP was determined by corneal hydration values, Draize score, aqueous humor protein concentration, corneal endothelial evaluation, as well as light microscopy and electron microscopy.

Results: The application of 0.2% SP-L and 0.2% SP-H to the cornea in vitro increased puerarin apparent permeability coefficient by 1.96-fold (P<0.05) and 2.95-fold (P<0.01), respectively. SP-H showed stronger effect than SP-L (P<0.05). For the in vivo assay, those were 1.81-fold (P<0.05) and 3.71-fold (P<0.01), respectively. With the SP application, the corneal hydration values were <83% and Draize scores were <4, with no apparent changes in histological observations.

Conclusion: SP is one potential adjuvant promoting puerarin permeability to the cornea, and the high-content amino residue SP showed stronger effect, without ocular toxicity.

MeSH terms

  • Adjuvants, Pharmaceutic / chemistry*
  • Adjuvants, Pharmaceutic / toxicity
  • Animals
  • Aqueous Humor / drug effects
  • Aqueous Humor / metabolism
  • Cell Count
  • Chromatography, High Pressure Liquid
  • Cornea / drug effects*
  • Cornea / metabolism
  • Data Interpretation, Statistical
  • Endothelial Cells / diagnostic imaging
  • Endothelial Cells / drug effects
  • Endothelium, Corneal / diagnostic imaging
  • Endothelium, Corneal / drug effects
  • Endothelium, Corneal / metabolism
  • Eye Proteins / metabolism
  • Glucans / chemistry*
  • Glucans / toxicity
  • In Vitro Techniques
  • Isoflavones / administration & dosage
  • Isoflavones / chemistry
  • Isoflavones / pharmacokinetics*
  • Microscopy, Electron, Transmission
  • Molecular Structure
  • Ophthalmic Solutions
  • Rabbits
  • Spermine / chemistry*
  • Tissue Distribution
  • Ultrasonography

Substances

  • Adjuvants, Pharmaceutic
  • Eye Proteins
  • Glucans
  • Isoflavones
  • Ophthalmic Solutions
  • Spermine
  • pullulan
  • puerarin