A cationic iridium(III) complex showing aggregation-induced phosphorescent emission (AIPE) in the solid state: synthesis, characterization and properties

Dalton Trans. 2012 Jan 14;41(2):523-30. doi: 10.1039/c1dt11215e. Epub 2011 Nov 1.

Abstract

We report the synthesis and characterization of two cationic iridium(III) complexes with dendritic carbazole ligands as ancillary ligands, namely, [Ir(ppy)(2)L3]PF(6) (1) and [Ir(ppy)(2)L4]PF(6) (2), where L3 and L4 represent 3,8-bis(3,6-di-tert-butyl-9H-carbazol-9-yl)-1,10-phenanthroline and 3,8-bis(3',6'-di-tert-butyl-6-(3,6-di-tert-butyl-9H-carbazol-9-yl)-3,9'-bi(9H-carbazol)-9-yl)-1,10-phenanthroline, respectively. Their photophysical properties have been investigated and compared. The results have shown that complex 2 is aggregation-induced phosphorescent emission (AIPE) active and exhibits the highest photoluminescent quantum yield (PLQY) of 16.2% in neat film among the reported cationic Ir(III) complexes with AIPE activity. In addition, it also enjoys redox reversibility, good film-forming ability, excellent thermal stability as well as off/on luminescence switching properties, revealing its potential application as a candidate for light-emitting electrochemical cells and organic vapor sensing. To explore applications in biology, 2 was used to image cells.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Carbazoles / chemistry*
  • Cations
  • Cell Line, Tumor
  • Coordination Complexes / chemical synthesis*
  • Coordination Complexes / chemistry
  • Electrochemistry
  • Humans
  • Iridium / chemistry*
  • Ligands
  • Luminescence
  • Luminescent Measurements
  • Magnetic Resonance Spectroscopy
  • Microscopy, Atomic Force
  • Models, Chemical
  • Molecular Structure
  • Oxidation-Reduction
  • Photochemistry
  • Quantum Theory
  • X-Ray Diffraction

Substances

  • Carbazoles
  • Cations
  • Coordination Complexes
  • Ligands
  • Iridium