[Analysis of flavonoids in platycladi cacumen by UPLC-MS]

Zhongguo Zhong Yao Za Zhi. 2011 Jun;36(12):1626-9.
[Article in Chinese]

Abstract

Objective: To investigate the flavonoids in Platycladi Cacumen.

Method: The constituents in Platycladi Cacumen were determined by UPLC-MS. A Waters BEH C18 column (2.1 mm x 150 mm, 1.7 microm) was used with a gradient elution of methanol-water containing 0.2% formic acid. The mass spectrometer equipped with electrospay ionization source was used as defector and operated in data was collected under the negative ion modes.

Result: Eleven constituents were identified.

Conclusion: In this study, the main flavonoids in Platycladi Cacumen were separated by UPLC, and identified through the information of mass number and UV spectra. With the information of MS/MS from flavonoids, the modes of breaking up flavonoids were discussed. It is an accurate and effective method which can be applied for the constituent identification of Platycladi Cacumen.

Publication types

  • English Abstract

MeSH terms

  • Chromatography, Liquid / methods*
  • Cupressaceae / chemistry*
  • Flavonoids / chemistry*
  • Mass Spectrometry / methods*
  • Plant Extracts / chemistry*

Substances

  • Flavonoids
  • Plant Extracts