Efficient synthesis of esermethole and its analogues

Org Biomol Chem. 2011 Jun 7;9(11):4091-7. doi: 10.1039/c1ob05275f. Epub 2011 Apr 7.

Abstract

In this work, a general and flexible synthetic route towards the synthesis of pyrroloindoline alkaloids was developed. This new strategy features with a palladium mediated sequential arylation-allylation of o-bromoanilides and leads to the construction of oxindoles bearing a full carbon quaternary center. The cheap triphenylphosphine was proved to be a highly effective ligand for this one pot transformation. On the basis of this new method, esermethole and its analogues were synthesized.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Molecular Structure
  • Physostigmine / analogs & derivatives*
  • Physostigmine / chemical synthesis
  • Physostigmine / chemistry
  • Stereoisomerism

Substances

  • esermethole
  • Physostigmine