Water-soluble MnO nanocolloid for a molecular T1 MR imaging: a facile one-pot synthesis, in vivo T1 MR images, and account for relaxivities

ACS Appl Mater Interfaces. 2010 Oct;2(10):2949-55. doi: 10.1021/am100641z.

Abstract

A facile one-pot synthesis of a water-soluble MnO nanocolloid (i.e., D-glucuronic acid-coated MnO nanoparticle) is presented. The MnO nanoparticle in the MnO nanocolloid was coated with a biocompatible and hydrophilic D-glucuronic acid, and its particle diameter was nearly monodisperse and ranged from 2 to 3 nm. The average hydrodynamic diameter of the MnO nanocolloid was estimated to be 5 nm. The MnO nanoparticle was nearly paramagnetic down to T=3 K. The MnO nanocolloid showed a high longitudinal water proton relaxivity of r1=7.02 s(-1) mM(-1) with the r2/r1 ratio of 6.83 due to five unpaired S-state electrons of Mn(II) ion (S=5/2) as well as a high surface to volume ratio of the MnO nanoparticle. High contrast in vivo T1 MR images were obtained for various organs, showing the capability of the MnO nanocolloid as a sensitive T1 MRI contrast agent. The suggested three key-parameters which control the r1 and r2 relaxivities of nanocolloids (i.e., the S value of a metal ion, the spin structure, and the surface to volume ratio of a nanoparticle) successfully accounted for the observed r1 and r2 relaxivities of the MnO nanocolloid.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Colloids
  • Contrast Media / chemistry*
  • Glucuronic Acid / chemistry*
  • Magnetic Resonance Imaging*
  • Manganese Compounds / chemistry*
  • Nanoparticles / chemistry*
  • Oxides / chemistry*
  • Solubility

Substances

  • Colloids
  • Contrast Media
  • Manganese Compounds
  • Oxides
  • manganese oxide
  • Glucuronic Acid